论文标题

多层锡/Al $ _2 $ o $ _3 $传输dynodes的二级电子排放

Secondary Electron Emission from Multi-layered TiN/Al$_2$O$_3$ Transmission Dynodes

论文作者

Chan, H. W., Prodanović, V., Theulings, A. M. M. G., Hagen, C. W., Sarro, P. M., Graaf, H. v. d

论文摘要

多层Al $ _2 $ o $ _3 $/锡膜的(次级)电子发射已在扫描电子显微镜中使用半球收集器系统进行了研究,该电子显微镜的能量在0.3至10 keV之间。这些超薄的膜被设计为在新型真空电子乘数中充当传输点。两种不同类型的双层和三层,已通过氧化铝氧化铝的原子层沉积(ALD)和硝酸钛溅射制造。两种类型的膜的反射和传输电子产量($σ_R$,$σ_T$)均已测量。相比之下,三层膜在具有相同有效厚度的膜的透射电子产率方面优于双层膜。最高的传输电子产量以Al $ _2 $ o $ _3 $ _3 $ _3 $ _3 $/al $ _2 $ o $ _3 $胶片为5/2.5/5 nm的胶卷,其最大变速器电子产量$σ_\ text {t}^\ text {t}^\ text {max}(e_0)$ 3.1(e_0)$ 3.1(1.55 kev)。此外,通过使用正样品偏置进行额外的测量来分离发射分数$η_t$和传输二级电子产率$Δ_T$,对双层膜进行了更深入的研究。传输分数用于确定传输参数$ p $,该参数表征了薄膜中主要电子(PE)的相互作用。传输二级电子产率用于比较厚度不同的膜中PE的能量传递。

The (secondary) electron emission from multilayered Al$_2$O$_3$/TiN membranes has been investigated with a hemispherical collector system in a scanning electron microscope for electrons with energies between 0.3 and 10 keV. These ultra-thin membranes are designed to function as transmission dynodes in novel vacuum electron multipliers. Two different types, a bi-layer and a tri-layer, have been manufactured by means of atomic-layer deposition (ALD) of aluminum oxide and sputtering of titanium nitride. The reflection and transmission electron yield ($σ_R$, $σ_T$) have been measured for both types of membranes. In comparison, the tri-layer membranes outperformed the bi-layer membranes in terms of transmission electron yield for films with the same effective thickness. The highest transmission electron yield was measured on an Al$_2$O$_3$/TiN/Al$_2$O$_3$ film with layer thicknesses of 5/2.5/5 nm, which had a maximum transmission electron yield $σ_\text{T}^\text{max}(E_0)$ of 3.1 (1.55 keV). Furthermore, the bi-layer membranes have been investigated more in-depth by performing an additional measurement using a positive sample bias to separate the transmitted fraction $η_T$ and the transmission secondary electron yield $δ_T$. The transmitted fraction was used to determine the transmission parameter $p$, which characterizes the interaction of primary electrons (PEs) in thin films. The transmission secondary electron yield was used to compare the energy transfer of PEs in films with different thicknesses.

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