论文标题

由激光粉床融合印刷的hastelloy-X合金的微裂缝,微结构和机械性能:建造,退火和静置的抑制作用

Micro-cracking, microstructure and mechanical properties of Hastelloy-X alloy printed by laser powder bed fusion: as-built, annealed and hot-isostatic pressed

论文作者

Wang, Hui, Chen, Liu, Dovgyy, Bogdan, Xu, Wenyong, Sha, Aixue, Li, Xingwu, Tang, Huiping, Liu, Yong, Wu, Hong, Pham, Minh-Son

论文摘要

这项研究分析了文献数据,以识别优化的打印参数,并评估由激光粉末床融合打印的Hastelloy-X的合并,微结构和机械性能。还揭示了退火后和热相分化压力(HIP)对微结构和机械性能的影响。通过计算热力学相图,可以预测对凝固破裂和诸如降水和化学分离等固化的微观结构的敏感性。在整个构建过程中的固化裂纹分布被量化,以供建造,退火和髋关节条件。评估揭示了底部,顶部和自由表面的裂纹密度的变化。发现裂纹的分布与通过分析热计算估计的热梯度和热导率相关。虽然退火和臀部都可以通过恢复和重结晶可以改变当然的微观结构,但仅臀部才能成功地去除微裂缝和毛孔。除了去除外,髋关节的重结晶和沉淀(比退火更强),从而获得最佳的机械性能,包括从13%的13%伸长率将大幅增加到20%,这显着提高了965 MPA的最终拉伸应力,从965 MPA增加到1045 MPa,伴有中等高的屈服应力,这要归功于降水量。

This study analyses literature data to identify optimised print parameters and assesses the consolidation, microstructure, and mechanical properties of Hastelloy-X printed by laser powder bed fusion. Effects of post annealing and hot-isostatic pressing (HIP) on the microstructure and mechanical properties are also revealed. The susceptibility to the solidification cracking and the as-built microstructure such as precipitation and chemical segregation were predicted by the calculation of thermodynamics phase diagrams. The distribution of solidification cracks throughout the builds was quantified for the as-built, annealed and HIP conditions. The assessment reveals the variation of crack density towards the bottom, top and free surface of solid builds. This distribution of cracks is found to be associate with the thermal gradient and thermal conductivity which were estimated by analytical thermal calculations. While the annealing and HIP both can alter the as-printed microstructure thanks to recovery and recrystallisation, the micro-cracks and pores were only successfully removed by the HIP. In addition to the removal, recrystallisation and precipitation in the HIP (stronger than in annealing), resulting in optimal mechanical properties including a substantial increase in elongation from 13% to 20%, significant improvement of ultimate tensile stress from 965 MPa to 1045 MPa with moderately high yield stress thanks to precipitation.

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